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The combined organic layer was washed with brine, dried with sodium sulfate, filtered and concentrated under reduced pressure, and the residue was triturated with toluene for 1 h. The resulting off-white solid was isolated by filtration to give the desired product (1.37 g, 77%) as an off-white solid.
For these situations, high efficiency cyclonic collectors can achieve up to 85 percent control of paniculate. Under normal firing conditions, or when a clean oil is combusted, cyclonic collectors are not nearly so effective because of the high percentage of small particles (less than 3 micrometers in diameter) emitted. 7/93 External Combustion
Sodium sulfate (Na2S04), resulting from oxidation in the absorber, is purged from the absorber product solution, crystallized and sold. The remaining sodium bisulfite (NaHS03) solution is evaporated and the resultant crystals thermally decomposed to give sodium sulfite (Na2S03) and gaseous S02.
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